Réaction #71571

Équation de réaction

dimethyl sulfide

methyltrifluoromethane sulfonate

→

Trimethylsulfonium Triflate

Solvants

dichloromethane

Conditions de réaction

Traitement

1. 1
   Autreto obtain a white solid product
2. 2
   FiltrationThe solid product was filtered
3. 3
   Autredried for 1 hour in an oven at 50° C.
4. 4
   Autreto obtain the following product

Mode opératoire

16 mmol of dimethyl sulfide was dissolved in 10 ml of dichloromethane at 0° C., and about 17 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture to obtain a white solid product. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:

Source