Réaction #6820

ord-20d2e46c1d1247a2976c93d528f9a3be

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Traitement

  1. 1
    AutreThe volatile materials were evaporated

Mode opératoire

A solution of (4-phenyl-but-3-ynyl)-carbamic acid tert-butyl ester (98 mg) was stirred for 0.5 h in 1:1 trifluoroacetic acid/dichloromethane (10 ml). The volatile materials were evaporated to give the crude 4-phenyl-but-3-ynylamine, which was used in subsequent transformations without further purification.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US07084154B2uspto-grants-2006_08