Réaction #6683

Équation de réaction

[R]-1-trifluoromethylheptyl 4-benzyloxybenzoate

→

[R]-1-Trifluoromethylheptyl 4-hydroxybenzoate

Rendement 99.0%

Solvants

ethyl acetate

Conditions de réaction

Traitement

1. 1
   FiltrationThen the catalyst was filtered out
2. 2
   Autrefiltrate was evaporated to dryness
3. 3
   Autreto give the pure compound in yield of 99%

Mode opératoire

2.2 g of [R]-1-trifluoromethylheptyl 4-benzyloxybenzoate, (13) 100 mg of PdOH/C in 50 ml of ethyl acetate was stirred at RT over night under H2 atmosphere. Then the catalyst was filtered out and filtrate was evaporated to dryness to give the pure compound in yield of 99%.

Source