Réaction #66010

Équation de réaction

allyl bromide

diethylene glycol

→

Diethylene glycol monoallyl ether

Rendement 82.0%

Solvants

THF NaH

Conditions de réaction

Traitement

1. 1
   AutreThe product was obtained in 82% yield
2. 2
   workup.DISTILLATIONafter distillation

Mode opératoire

Diethylene glycol monoallyl ether was prepared by reacting allyl bromide with excess diethylene glycol in THF-NaH (tetrahydrofuran-sodium hydride). The product was obtained in 82% yield after distillation. b.p.=96-99° C./7 mmHg.

Source