Réaction #58265

ord-e4a6a69cc04848b1bbcf385a656798d5

Équation de réaction

COc1ccc(C(=O)c2ccc(Cl)cc2)c(C(=O)O)c1
2-(4-chlorobenzoyl)-5-methoxybenzoic acid
NN.O
hydrazine hydrate
→
COc1ccc2c(-c3ccc(Cl)cc3)n[nH]c(=O)c2c1
4-(4-Chlorophenyl)-7-methoxy-2H-phthalazin-1-one

Réactifs

COc1ccc(C(=O)c2ccc(Cl)cc2)c(C(=O)O)c1
2-(4-chlorobenzoyl)-5-methoxybenzoic acid
NN.O
hydrazine hydrate

Réactifs

Aucun

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Traitement

  1. 1
    AutreThis compound is obtained

Mode opératoire

This compound is obtained according to the procedure described in 1.2. by reacting 2-(4-chlorobenzoyl)-5-methoxybenzoic acid unpurified with hydrazine hydrate.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US07423030B2uspto-grants-2008_09