Réaction #573436

ord-2df2766700ed406bba7639e5b14b0a74

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Traitement

  1. 1
    Températurethe mixture is refluxed for hour
  2. 2
    ConcentrationAfter concentrating

Mode opératoire

To 2-methyl-3,4,6-trifluorobenzoic acid (3.2 g) is added thiony chloride (7 ml) and the mixture is refluxed for hour. After concentrating, 2-methyl-3,4,6-trifluorobenzoyl chloride (3.3 g) is obtained.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US05290934uspto-grants-1994_03