Réaction #56521

Équation de réaction

isoamyl nitrite

benzene

2,4-difluoroaniline

→

2,4-difluorobiphenyl

Conditions de réaction

Traitement

1. 1
   Températurethermometer, nitrogen-inlet, internal steam coil and reflux condenser

Mode opératoire

To a 50 liter resin pot equipped with stirrer, thermometer, nitrogen-inlet, internal steam coil and reflux condenser is charged 31.5 liters of benzene, 1.025 liters of isoamyl nitrite and 700 g. (5.43 moles) of 2,4-difluoroaniline.

Source