Réaction #55653

ord-0b28560bfaca4bedaf9fde88729ace75

Équation de réaction

O=C(O)CC(CCCc1ccc(O)cc1)CC(=O)O
3-[3-(4-Hydroxyphenyl)propyl]glutaric acid
CC(=O)OC(C)=O
acetic anhydride
→
CC(=O)Oc1ccc(CCCC2CC(=O)OC(=O)C2)cc1
3-[3-[4-(acetyloxy)phenyl]propyl]glutaric anhydride

Réactifs

O=C(O)CC(CCCc1ccc(O)cc1)CC(=O)O
3-[3-(4-Hydroxyphenyl)propyl]glutaric acid
CC(=O)OC(C)=O
acetic anhydride

Réactifs

Aucun

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

3-[3-(4-Hydroxyphenyl)propyl]glutaric acid (533 mg) is reacted with acetic anhydride as described in Example 1C to afford 3-[3-[4-(acetyloxy)phenyl]propyl]glutaric anhydride, melting point 55°-57° C.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US04221725uspto-grants-1980_09