Réaction #54974

ord-a79709e505384a2687bef6e5cd029a87

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

0.1 mole resorcinol and 0.1 mole ethyl acetylacetate in solution in 100 ml concentrated sulphuric acid are maintained at 5° C. for 3 hours. After recyrstallisation of the solid formed from ethanol, there are obtained 12.5 grams 4-methyl-7-hydroxy-coumarin, melting at 185° C.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US04151291uspto-grants-1979_04