Réaction #51741

Équation de réaction

2-(methyloxycarbonyl)amino-4-isopropyl-7-methyl-6-thiocyanato-benzothiazole

dithiothreitol

phosphate

→

title compound

2-(Methyloxycarbonyl)amino-4-isopropyl-7-methyl-benzothiazole-6-thiol

Solvants

EtOH

Conditions de réaction

Mode opératoire

The title compound was prepared according to General Method 14 using 2-(methyloxycarbonyl)amino-4-isopropyl-7-methyl-6-thiocyanato-benzothiazole (1.5 g, 4.7 mmol), dithiothreitol (2.9 g, 18.7 mmol), EtOH (50 mL), and phosphate buffer (15 mL). MS (APCI): 296 (M−H).

Source