Réaction #5127
ord-4bb73f6b08114a6bb1231cd70986f4d3
Équation de réaction
1,17-biscyclohexylguanidino-9-azaheptadecane dihydroiodide
methanol water
→
guanidine
1,17-Biscyclohexylguanidino-9-azaheptadecane triacetate
Réactifs
Aucun
Conditions de réaction
Conditions détaillées
See reaction.notes.procedure_details.
Mode opératoire
10.2 g (0.011 mol) of 1,17-biscyclohexylguanidino-9-azaheptadecane dihydroiodide in 150 ml of methanol/water (1:1) were filtered through a column containing 250 g of ion exchanger (OH- form). The free guanidine base obtained after working up was dissolved in methanol and converted into the triacetate with excess glacial acetic acid.