Réaction #502164

ord-cbfe5ed99dbd4ccb873ed01a5a53db2b

Équation de réaction

CSc1nc(Cc2ccsc2)[nH]c(=O)c1C#N
4-(methylsulphanyl)-6-oxo-2-(3-thienylmethyl)-1,6-dihydropyrimidine-5-carbonitrile
CC(C)(C)C1CCNCC1
4-tert-butylpiperidine
CC(C)(C)C1CCN(c2nc(Cc3ccsc3)[nH]c(=O)c2C#N)CC1
title compound
CC(C)(C)C1CCN(c2nc(Cc3ccsc3)[nH]c(=O)c2C#N)CC1
4-[4-(tert-Butyl)piperidin-1-yl]-6-oxo-2-(3-thienylmethyl)-1,6-dihydropyrimidine-5-carbonitrile

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

In analogy to the preparation of Example 1, 100 mg (0.38 mmol) of 4-(methylsulphanyl)-6-oxo-2-(3-thienylmethyl)-1,6-dihydropyrimidine-5-carbonitrile are reacted with 536 mg (3.80 mmol) of 4-tert-butylpiperidine to give 57 mg (42% of theory) of the title compound.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US08088769B2uspto-grants-2012_01