Réaction #502163

ord-70558a5718784a1f8ac920042e608df0

Équation de réaction

CSc1nc(Cc2ccsc2)[nH]c(=O)c1C#N
4-(methylsulphanyl)-6-oxo-2-(3-thienylmethyl)-1,6-dihydropyrimidine-5-carbonitrile
CC1(C)CCNCC1
4,4-dimethylpiperidine
CC1(C)CCN(c2nc(Cc3ccsc3)[nH]c(=O)c2C#N)CC1
title compound
CC1(C)CCN(c2nc(Cc3ccsc3)[nH]c(=O)c2C#N)CC1
4-(4,4-Dimethylpiperidin-1-yl)-6-oxo-2-(3-thienylmethyl)-1,6-dihydropyrimidine-5-carbonitrile

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

In analogy to the preparation of Example 1, 100 mg (0.38 mmol) of 4-(methylsulphanyl)-6-oxo-2-(3-thienylmethyl)-1,6-dihydropyrimidine-5-carbonitrile are reacted with 430 mg (3.80 mmol) of 4,4-dimethylpiperidine to give 42 mg (34% of theory) of the title compound.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US08088769B2uspto-grants-2012_01