Réaction #502153

ord-d63653e7c1aa48258c90c62f468293d3

Équation de réaction

CSc1nc(Cc2ccc(Cl)cc2)[nH]c(=O)c1C#N
2-(4-chlorobenzyl)-4-(methylsulphanyl)-6-oxo-1,6-dihydropyrimidine-5-carbonitrile
NC1CCC1
cyclobutylamine
N#Cc1c(NC2CCC2)nc(Cc2ccc(Cl)cc2)[nH]c1=O
title compound
N#Cc1c(NC2CCC2)nc(Cc2ccc(Cl)cc2)[nH]c1=O
2-(4-Chlorobenzyl)-4-(cyclobutylamino)-6-oxo-1,6-dihydropyrimidine-5-carbonitrile

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

In analogy to the preparation of Example 1, 100 mg (0.34 mmol) of 2-(4-chlorobenzyl)-4-(methylsulphanyl)-6-oxo-1,6-dihydropyrimidine-5-carbonitrile are reacted with 244 mg (3.43 mmol) of cyclobutylamine to give 15 mg (14% of theory) of the title compound.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US08088769B2uspto-grants-2012_01