Réaction #502151

ord-78e3f54cb6394e8fa847ea1bceaf233a

Équation de réaction

CSc1nc(Cc2cccc(Cl)c2)[nH]c(=O)c1C#N
2-(3-chlorobenzyl)-4-(methylsulphanyl)-6-oxo-1,6-dihydropyrimidine-5-carbonitrile
CN1CCNCC1
N-methylpiperazine
CN1CCN(c2nc(Cc3cccc(Cl)c3)[nH]c(=O)c2C#N)CC1
title compound
CN1CCN(c2nc(Cc3cccc(Cl)c3)[nH]c(=O)c2C#N)CC1
2-(3-Chlorobenzyl)-4-(4-methylpiperazin-1-yl)-6-oxo-1,6-dihydropyrimidine-5-carbonitrile

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

In analogy to the preparation of Example 1, 100 mg (0.34 mmol) of 2-(3-chlorobenzyl)-4-(methylsulphanyl)-6-oxo-1,6-dihydropyrimidine-5-carbonitrile are reacted with 343 mg (3.43 mmol) of N-methylpiperazine to give 101 mg (84% of theory) of the title compound.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US08088769B2uspto-grants-2012_01