Réaction #48372

ord-85f631a64d1f456f809694e9f8f1ed62

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Traitement

  1. 1
    Autrethe volatiles were removed in vacuo

Mode opératoire

N-(3-Azido-5-fluoropyridin-2-yl)-2,2-dimethylpropanamide (275 mg, 1.16 mmol) in 3 N HCl (5 mL) was heated to 100° C. After 2 h, the volatiles were removed in vacuo, to give the title compound as its HCl salt (180 mg). MS154.2 (M+1).

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US07745427B2uspto-grants-2010_06