Réaction #475066

Équation de réaction

3-Methylthiopropylamine

hexane ethyl acetate

→

title compound

Rendement 93.1%

Phenyl N-(3-methylthiopropyl)carbamate

Rendement 93.1%

Conditions de réaction

Mode opératoire

3-Methylthiopropylamine (5.5 ml, 50 mmol) was used for reaction in the same manner as Production Example 310-1, and purification was performed by silica gel column chromatography (hexane/ethyl acetate system) to obtain the title compound (10.486 g, 46.54 mmol, 93.08%) as a yellow oil.

Source