Réaction #4723

ord-1dc6b5574bd346ad89e9cac4f2b34550

Équation de réaction

NNC(=S)NCCCOc1cccc(CN2CCCCC2)c1
N-[3-[3-(1-piperidinylmethyl) phenoxy]propyl]-hydrazine carbothioamide
ClC(Cl)=Nc1ccccc1
phenyl isocyanide dichloride
→
c1ccc(Nc2nnc(NCCCOc3cccc(CN4CCCCC4)c3)s2)cc1
N-Phenyl-N'-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]1,3,4-thiadiazole-2,5-diamine

Réactifs

NNC(=S)NCCCOc1cccc(CN2CCCCC2)c1
N-[3-[3-(1-piperidinylmethyl) phenoxy]propyl]-hydrazine carbothioamide
ClC(Cl)=Nc1ccccc1
phenyl isocyanide dichloride

Réactifs

Aucun

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

The compound is prepared by a method analogous to that of Example 29 from N-[3-[3-(1-piperidinylmethyl) phenoxy]propyl]-hydrazine carbothioamide and phenyl isocyanide dichloride. The analytical values are summarized in Table II.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US04727081uspto-grants-1988_02