Réaction #452433

Équation de réaction

4-dimethylamino-1-cyclohexanone ethylene ketal

→

title compound

Rendement 100.0%

4-dimethylamino-1-cyclohexanone

Rendement 100.0%

Solvants

formic acid

Conditions de réaction

Traitement

1. 1
   Températureat reflux for 18 hours
2. 2
   TempératureThe reaction mixture was then cooled to ambient and the volatiles
3. 3
   Autreremoved under reduced pressure

Mode opératoire

4.96 gm (26.8 mMol) 4-dimethylamino-1-cyclohexanone ethylene ketal were dissolved in 50 mL formic acid and the solution stirred at reflux for 18 hours. The reaction mixture was then cooled to ambient and the volatiles removed under reduced pressure to give 3.78 gm (100%) of the title compound.

Source