Réaction #443125

ord-78f5ec2787d6472997528e93e764da4c

Équation de réaction

CCCCCCCCCCCC(Br)Br
dibromododecane
Nc1ccc(-c2ccccc2)cn1
2-amino-5-phenylpyridine
→
Br.Br.N=c1ccc(-c2ccccc2)cn1CCCCCCCCCCCCn1cc(-c2ccccc2)ccc1=N
1,1'-(1,12-dodecanediyl)bis(5-phenyl-2(1H)-pyridinimine) dihydrobromide

Réactifs

CCCCCCCCCCCC(Br)Br
dibromododecane
Nc1ccc(-c2ccccc2)cn1
2-amino-5-phenylpyridine

Réactifs

Aucun

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Traitement

  1. 1
    AutreThe product obtained
  2. 2
    Autreis purified by recrystallization in methanol

Mode opératoire

The procedure is as before, with dibromododecane and 2-amino-5-phenylpyridine. The product obtained is purified by recrystallization in methanol. Its m.p.=185° C.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US05834491uspto-grants-1998_11