Réaction #417924

Équation de réaction

sodium hydroxide

29

methyl 2-(undec-4Z-enyloxy)benzoate

→

yellow oil

Rendement 99.5%

2-(undec-4Z-enyloxy)benzoic acid

Rendement 99.5%

Solvants

methanol

Conditions de réaction

Traitement

1. 1
   TempératureThe solution is refluxed for 24 hours
2. 2
   AutreAfter evaporating off the solvent
3. 3
   Extractionextracted with DCM

Mode opératoire

500 μL of 1 N sodium hydroxide solution (500 μmol) are added portionwise to 80 mg of 29 (263 μmol) in methanol (3 mL). The solution is refluxed for 24 hours. After evaporating off the solvent, the reaction medium is acidified with 0.5 N HCl and extracted with DCM. 76 mg of a yellow oil are obtained, i.e. a yield of 99%.

Source