Réaction #417906
ord-dd72aa198be14ac5966dd35f8a2286f6
Équation de réaction
Desmorapid
n-butyl isocyanate
isocyanate
→
Isopropyl butylcarbamate
Réactifs
Aucun
Solvants
Conditions de réaction
Température
60°CELSIUS
Conditions détaillées
See reaction.notes.procedure_details.
Traitement
- 1TempératureThereafter, cooling
- 2Autrethe product was obtained as a clear liquid
Mode opératoire
In a 250 ml round-bottomed flask, 0.02 g of Desmorapid Z, 31.1 g of n-butyl isocyanate were initially introduced and heated to 60° C. Thereafter, 18.9 g of isopropanol were added dropwise and the mixture was further kept at 60° C. until the isocyanate content had fallen below 0.1%. Thereafter, cooling was effected and the product was obtained as a clear liquid.