Réaction #417904
ord-9eb251ab9d2f4dd397596f5f2a9d6088
Équation de réaction
Desmorapid
n-hexyl isocyanate
isocyanate
→
Isopropyl hexylcarbamate
Réactifs
Aucun
Solvants
Conditions de réaction
Température
60°CELSIUS
Conditions détaillées
See reaction.notes.procedure_details.
Traitement
- 1TempératureThereafter, cooling
- 2Autrethe product was obtained as a clear liquid
Mode opératoire
In a 250 ml round-bottomed flask, 0.02 g of Desmorapid Z, 34.0 g of n-hexyl isocyanate were initially introduced and heated to 60° C. Thereafter, 16.0 g of isopropanol were added dropwise and the mixture was further kept at 60° C. until the isocyanate content had fallen below 0.1%. Thereafter, cooling was effected and the product was obtained as a clear liquid.