Réaction #417904

ord-9eb251ab9d2f4dd397596f5f2a9d6088

Équation de réaction

CN(C)CCCN1CN(CCCN(C)C)CN(CCCN(C)C)C1
Desmorapid
CCCCCCN=C=O
n-hexyl isocyanate
[N-]=C=O
isocyanate
CCCCCCNC(=O)OC(C)C
Isopropyl hexylcarbamate

Solvants

Conditions de réaction

Température
60°CELSIUS
Conditions détaillées
See reaction.notes.procedure_details.

Traitement

  1. 1
    TempératureThereafter, cooling
  2. 2
    Autrethe product was obtained as a clear liquid

Mode opératoire

In a 250 ml round-bottomed flask, 0.02 g of Desmorapid Z, 34.0 g of n-hexyl isocyanate were initially introduced and heated to 60° C. Thereafter, 16.0 g of isopropanol were added dropwise and the mixture was further kept at 60° C. until the isocyanate content had fallen below 0.1%. Thereafter, cooling was effected and the product was obtained as a clear liquid.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US08877408B2uspto-grants-2014_11