Réaction #41355

Équation de réaction

Sodium periodate

3-phenoxy-1,2-propanediol

→

subtitle compound

Rendement 100.0%

2-Phenoxyacetaldehyde

Rendement 100.0%

Solvants

dichloromethane

dichloromethane

Conditions de réaction

Traitement

1. 1
   Filtrationwas filtered
2. 2
   Concentrationthe filtrate was concentrated

Mode opératoire

Sodium periodate (0.65 M in water, 20 mL) was added to a vigorously stirred suspension of silica gel (20 g) in dichloromethane (160 mL), followed by a solution of 3-phenoxy-1,2-propanediol (1.68 g, 10.0 mmol) in dichloromethane (20 mL). After stirring for 10 min the mixture was filtered and the filtrate was concentrated to give the subtitle compound (1.36 g, 100%).

Source