Réaction #40329
ord-d3ec7ce35c5743429efed8cc6b073b42
Équation de réaction
8-(4-fluorophenyl)-1,4-dioxaspiro[4.5]dec-7-ene
hydrogen
→
8-(4-fluorophenyl)-1,4-dioxaspiro[4.5]decane
Réactifs
Conditions de réaction
Conditions détaillées
See reaction.notes.procedure_details.
Mode opératoire
8-(4-fluorophenyl)-1,4-dioxaspiro[4.5]dec-7-ene is hydrogenated using Pd/C with hydrogen. After filtering-off of the catalyst over celite and evaporating-off of the solvent, 8-(4-fluorophenyl)-1,4-dioxaspiro[4.5]decane is obtained in a quantitative yield: tR 3.65 min (LC-1); ESI-MS(+): m/z 237.26 [M+H]+.