Réaction #40287

ord-128be03e30fc479198b6496eaff8785b

Équation de réaction

CCOC(=O)CON
2-Aminoxy-acetic acid ethyl ester
C#CCCC(=O)O
4-Pentynoic acid
C(=NC1CCCCC1)=NC1CCCCC1
dicyclohexylcarbodiimide
C#CCCC(=O)NOCC(=O)OCC
Pent-4-ynoylaminooxy-acetic Acid Ethyl Ester

Solvants

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

To a solution of 2-Aminoxy-acetic acid ethyl ester (573 mg, 4.8 mmol) and 4-Pentynoic acid (441 mg, 4.5 mmol) in 15 mL EtOAc were added dicyclohexylcarbodiimide (928 mg, 4.5 mmol) and the resulting mixture was stirred at room temperature for 16 h.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US07727713B2uspto-grants-2010_06