Réaction #3847

ord-6da5e6fc912a4f39abb42807db3359a7

Équation de réaction

CN(c1ncc(Cl)cc1Cl)S(=O)(=O)c1ccccn1
N-methyl-N-(3,5-dichloro-2-pyridyl)-2-pyridinesulfonamide
CC(=O)OO
peracetic acid
→
CN(c1ncc(Cl)cc1Cl)S(=O)(=O)c1cccc[n+]1[O-]
title compound
CN(c1ncc(Cl)cc1Cl)S(=O)(=O)c1cccc[n+]1[O-]
N-methyl-N-(3,5-dichloro-2-pyridyl)-2-pyridinesulfonamide 1-oxide

Réactifs

CN(c1ncc(Cl)cc1Cl)S(=O)(=O)c1ccccn1
N-methyl-N-(3,5-dichloro-2-pyridyl)-2-pyridinesulfonamide
CC(=O)OO
peracetic acid

Réactifs

Aucun

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

Following the procedures of Example 1, N-methyl-N-(3,5-dichloro-2-pyridyl)-2-pyridinesulfonamide is oxidized with 40% peracetic acid to give the title compound, MS m/e 334.00 (M+).

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US04722749uspto-grants-1988_02