Réaction #343475

Équation de réaction

triethylene tetraamine

KOH

ethylene carbonate

→

ethylene carbonate triethylene tetraamine

Solvants

toluene

Conditions de réaction

Traitement

1. 1
   Autrefitted with a stirrer
2. 2
   TempératureReflux the system for 2.5 hours under N2

Mode opératoire

Add 2 g of triethylene tetraamine (with an AV of approximately 1180 mg KOH/g) to 20 ml of toluene in a 250 ml flask fitted with a stirrer, condensor and nitrogen inlet. Add 0.6 g ethylene carbonate to the mixture. Reflux the system for 2.5 hours under N2. Strip the system to yield an ethylene carbonate-triethylene tetraamine adduct having an AV of approximately 670 mg KOH/g.

Source