Réaction #342078

Équation de réaction

sodium hexafluorophosphate

N-methoxymethyl-N-methylpyrrolidinium chloride

dichloromethane

→

desired product

Rendement 70.1%

N-methoxymethyl-N-methylpyrrolidinium hexafluorophosphate

Rendement 70.1%

Solvants

water

Conditions de réaction

Traitement

1. 1
   Autreto obtain a white solid
2. 2
   LavageThe extract was washed with 20 g of water 15 times
3. 3
   Autredried

Mode opératoire

In 120 g of water was dissolved 20.0 g of N-methoxymethyl-N-methylpyrrolidinium chloride and thereto was added 20.3 g of sodium hexafluorophosphate to obtain a white solid. The mixture was stirred for 30 minutes, and dichloromethane was added to the mixture for extraction. The extract was washed with 20 g of water 15 times, thereafter dried, giving 23.3 g of the desired product in the form of a white solid.

Source