Réaction #336822
ord-5ef4352b11c3443e87db73d3185b8e02
Équation de réaction
3,7-dimethyl-1-octanol
ethyl lactate
→
3,7-dimethyl-1-octyl lactate
Rendement 62.2%
Réactifs
Aucun
Conditions de réaction
Température
60°CELSIUS
Conditions détaillées
See reaction.notes.procedure_details.
Mode opératoire
A mixture of Novozym 435 (2.81 g), molecular sieves (23.17 g), 3,7-dimethyl-1-octanol (4.64 g), and ethyl lactate (14.78 g) in a 250 mL beaker was maintained at 60° C. in a convection oven for 28 hours. Upon work-up, 4.2 g of 3,7-dimethyl-1-octyl lactate (62% yield) was obtained as an amber-colored liquid. The purity of the product was >96% as assessed by HPLC-RI.