Réaction #335006

ord-582a8a39dcd348d195f6f383bef92f05

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

In a process analogous to Example 7, using (±)-[2-[[2,6-bis(1-methylethyl)phenyl]amino]-2-oxoethyl]phenyl phosphinic acid in place of (±)-[2-[[2,6-bis(1-methylethyl)phenyl]amino]-2-oxoethyl]phosphonic acid, ethyl ester and 1-dodecanol in place of 1-nonanol, the title compound is obtained as a sticky white solid; mp 66°-68° C.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US05208224uspto-grants-1993_05