Réaction #3064

ord-2f2ad81b1f6b433ea7c984999ad32978

Solvants

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

To a mixture of 1 mmol of phenylalanine methyl ester hydrochloride and 2 mmol of triethylamine in 1 mL of DMF at 0 ° C. was added 2 mL of formic acid and 0.7 mL of acetic anhydride. After stirring for 16 h at rt, extractive isolation provided N-formylphenylalanine methyl ester.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US05731432uspto-grants-1998_03