Réaction #2931

Équation de réaction

water

1-(3-Furyl)-1-(4-methyl-5-oxazolyl)ethanol

Trimethylsilylazide

boron trifluoride

→

title compound

1-Azido-1-(3-furyl)-1-(4-methyl-5-oxazolyl)ethane

Solvants

benzene

Conditions de réaction

Traitement

1. 1
   Extractionextracted

Mode opératoire

1-(3-Furyl)-1-(4-methyl-5-oxazolyl)ethanol (1 g) was suspended in benzene (4 ml). Trimethylsilylazide (822 μl) was added followed by boron trifluoride diethyletherate (770 μl). The mixture was stirred overnight at room temperature, then poured into water and extracted to give the title compound.

Source