Réaction #2467932

ord-1931052940a24382be4e0266350ed35a

Équation de réaction

[Na+].[OH-]
sodium hydroxide
Nc1nc(N)nc(N)n1
melamine
COC(C=O)OC
dimethoxyethanal
COC(C=O)OC.Nc1nc(N)nc(N)n1
Melamine Dimethoxyethanal

Conditions de réaction

Température
52.5°CELSIUS
Conditions détaillées
See reaction.notes.procedure_details.

Traitement

  1. 1
    TempératureThis mixture was heated
  2. 2
    Températurewhile maintaining the pH
  3. 3
    Autreclose to 9-9.5 with adjustment

Mode opératoire

200 g of melamine (1.59 mol) were added to 660 g of a 60% aqueous solution of dimethoxyethanal (3.81 mol). This mixture was heated under stirring for 2 h at 50-55° C. while maintaining the pH close to 9-9.5 with adjustment, if necessary, with as much 20% sodium hydroxide as was required (about 7 g).

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US08257832B2uspto-grants-2012_09