Réaction #2384790

ord-818d695750fd48489a207ea31713dae7

Équation de réaction

CC1=NCCc2ccccc21
1-Methyl-3,4-dihydroisoquinoline
CI
iodomethane
→
CC1=[N+](C)CCc2ccccc21.[I-]
crystals
CC1=[N+](C)CCc2ccccc21.[I-]
1,2-Dimethyl-3,4-dihydroisoquinolinium Iodide

Réactifs

CC1=NCCc2ccccc21
1-Methyl-3,4-dihydroisoquinoline
CI
iodomethane

Réactifs

Aucun

Solvants

CC(C)=O
acetone

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

1-Methyl-3,4-dihydroisoquinoline (780 mg) was dissolved in acetone (7 ml) and iodomethane (0.38 ml) added. The solution was allowed to stand overnight at room temperature. The product was obtained as pale yellow crystals (1.4 g).

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US06492378B1uspto-grants-2002_12