Réaction #2383779
ord-c9005bbd285f49f68ba1a6be71d2b91f
Équation de réaction
Réactifs
Aucun
Solvants
Conditions de réaction
Conditions détaillées
See reaction.notes.procedure_details.
Traitement
- 1Températurecooling
Mode opératoire
Pentafluorobenzenesulfonyl chloride (25 g) was dissolved in 100 ml of methanol with ice-cooling, and 100 g of a 25% aqueous solution of tetramethylammonium hydroxide was gradually added thereto. The reaction mixture was stirred at room temperature for 3 hours, thereby a solution of a pentafluorobenzenesulfonic acid tetramethylammonium salt was obtained. This solution was used for salt exchange of a sulfonium salt and an iodonium salt.