Réaction #2358451

Équation de réaction

thionyl chloride

2-methyl-3,4,6-trifluorobenzoic acid

→

2-methyl-3,4,6-trifluorobenzoyl chloride

Conditions de réaction

Traitement

1. 1
   Températureby heating
2. 2
   Températurerefluxing for 1 hour
3. 3
   ConcentrationThe reaction mixture was concentrated

Mode opératoire

7 ml of thionyl chloride was added to 3.2 g of 2-methyl-3,4,6-trifluorobenzoic acid, followed by heating and refluxing for 1 hour. The reaction mixture was concentrated, giving 3.3 g of 2-methyl-3,4,6-trifluorobenzoyl chloride. Then 5 ml of toluene was added to the resulting 2-methyl-3,4,6-trifluorobenzoyl chloride to give a toluene solution.

Source