Réaction #2161236

Équation de réaction

thioanisole

dimethyl sulfate

water

→

Dimethylphenylsulfonium Hydrogen Sulfate

Solvants

diethyl ether

Conditions de réaction

Traitement

1. 1
   Autreseparated into two layers

Mode opératoire

6.2 g (0.05 mole) of thioanisole and 6.9 g (0.055 mole) of dimethyl sulfate were stirred for 12 hours at room temperature. 100 g of water and 50 ml of diethyl ether were added to the reaction solution whereupon the mixture separated into two layers. The aqueous layer was taken out, which was an aqueous solution of the target compound, dimethylphenylsulfonium hydrogen sulfate.

Source