Réaction #1994263

ord-267d28b583e342eabe45e36e095a86df

Équation de réaction

C[N+](C)(C)Cc1ccccc1.O=S(=O)([O-])C(F)(F)C(O)C(F)(F)F
Benzyltrimethylammonium 1,1,3,3,3-pentafluoro-2-hydroxypropane-1-sulfonate
O=C(Cl)C12CC3CC(CC(C3)C1)C2
1-adamantanecarboxylic acid chloride
→
C[N+](C)(C)Cc1ccccc1.O=C(OC(C(F)(F)F)C(F)(F)S(=O)(=O)[O-])C12CC3CC(CC(C3)C1)C2
benzyltrimethylammonium 2-(adamantane-1-carbonyloxy)-1,1,3,3,3-pentafluoropropane-1-sulfonate

Réactifs

C[N+](C)(C)Cc1ccccc1.O=S(=O)([O-])C(F)(F)C(O)C(F)(F)F
Benzyltrimethylammonium 1,1,3,3,3-pentafluoro-2-hydroxypropane-1-sulfonate
O=C(Cl)C12CC3CC(CC(C3)C1)C2
1-adamantanecarboxylic acid chloride

Réactifs

Aucun

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Traitement

  1. 1
    Autrewere reacted in accordance with the teaching of JP-A 2008-106045

Mode opératoire

Benzyltrimethylammonium 1,1,3,3,3-pentafluoro-2-hydroxypropane-1-sulfonate in Synthesis Example 1-1 and 1-adamantanecarboxylic acid chloride were reacted in accordance with the teaching of JP-A 2008-106045, yielding the desired compound, benzyltrimethylammonium 2-(adamantane-1-carbonyloxy)-1,1,3,3,3-pentafluoropropane-1-sulfonate as white crystals.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US08597869B2uspto-grants-2013_12