Réaction #1904041
ord-5e11c941b17046ef94b03835ee80a6cd
Équation de réaction
p-bromophenol
benzyl bromide
→
4-benzyloxybromobenzene
Réactifs
Aucun
Solvants
Conditions de réaction
Température
80°CELSIUS
Conditions détaillées
See reaction.notes.procedure_details.
Traitement
- 1workup.ADDITIONwere added
Mode opératoire
To a solution composed of p-bromophenol (17.3 g, 0.1 mol) and dry DMF (100 mL), anhydride K2CO3 (8.28 g, 0.06 mmol) and benzyl bromide (25.6 g, 0.15 mmol) were added. The mixture was stirred at 80° C. under a nitrogen atmosphere for six hours. Then, the reaction mixture was charged into 500 mL of ice water.