Réaction #1803430

Équation de réaction

2-(benzo[d]thiazol-2-ylthio)acetic acid

2,3,4,5-tetrahydro-1H-benzo[b]azepine

2,3,4,5-Tetrahydro-1H-benzo[b]azepine

→

45

Rendement 23.0%

2-(Benzothiazol-2-ylsulfanyl)-1-(2,3,4,5-tetrahydro-benzo[b]-azepin-1-yl)-ethanone

Rendement 23.0%

Conditions de réaction

Traitement

1. 1
   AutreThe title compound was synthesized

Mode opératoire

The title compound was synthesized according to General Procedure B using 2-(benzo[d]thiazol-2-ylthio)acetic acid and 2,3,4,5-tetrahydro-1H-benzo[b]azepine (6) to yield 45 as a white solid (23%): MS m/z: 355 (M+H)+. Anal. Calcd. For, C19H18N2OS2: C, 64.38; H, 5.12; N, 7.90; S, 18.09. Found: C, 64.53; H, 5.06; N, 7.83; S, 17.93.

Source