Réaction #1726660

ord-7d7570892ebf418f905cbd5615a71312

Équation de réaction

CC(=O)O.CC(=O)O.[Pd]
palladium(II) acetate trimer
CCC(=O)O
propionic acid
CCC(=O)[O-].CCC(=O)[O-].[Pd+2]
Palladium(II) Propionate

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Traitement

  1. 1
    TempératureThe mixture was maintained at 40 degrees Celsius for 24 hours
  2. 2
    AutreExcess propionic acid was removed under vacuum at room temperature

Mode opératoire

5 gm commercial palladium(II) acetate trimer (Aldrich) was added to 40 g of propionic acid. The mixture was maintained at 40 degrees Celsius for 24 hours. Excess propionic acid was removed under vacuum at room temperature. The resulting yellow solid was used for making palladium inks.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US08110254B1uspto-grants-2012_02