Réaction #1700436

Équation de réaction

2-(2,4-dichlorophenyl)hexyl amine

N,N-dimethyl formamide azine

→

white solid

Rendement 125.7%

4-[2-(2,4-dichlorophenyl)hexyl]-1,2,4-triazole

Rendement 125.7%

Solvants

toluene

Conditions de réaction

Traitement

1. 1
   Températureis heated
2. 2
   Températureunder reflux for 16 hours
3. 3
   AutreThe solvent is evaporated

Mode opératoire

A mixture of 10 g (0.04 mole) of 2-(2,4-dichlorophenyl)hexyl amine, 5.7 g (0.04 mole) of N,N-dimethyl formamide azine and 0.5 g of p-toluene sulfonic acid in 100 ml of dry toluene is heated under reflux for 16 hours. The solvent is evaporated to give 15 g of a white solid which can be further purified by recrystallization from benzene to give 7.5 g of pure product.

Source