Réaction #1458415

ord-1bc0273f6d9e4898b5a2d888224182f6

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Traitement

  1. 1
    Autreused in Example 1 over a reaction period of 42 hours

Mode opératoire

The procedure of Example 1 was repeated except that 3 molar equivalents of p-chlorophenyl acetate (a conventional acylating agent) was used in place of isopropenyl acetate in the presence of three times the amount of the enzyme catalyst used in Example 1 over a reaction period of 42 hours, to obtain (R)-1-phenylethyl acetate having an optical purity of higher than 99%, at a yield of 95%.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US07156731B2uspto-grants-2007_01