Réaction #1369

Équation de réaction

2-methyl-3,4,6-trifluorobenzoic acid

chloride

→

2-methyl-3,4,6-trifluorobenzoyl chloride

Conditions de réaction

Traitement

1. 1
   Températurethe mixture is refluxed for 1 hour
2. 2
   ConcentrationAfter concentrating

Mode opératoire

To 2-methyl-3,4,6-trifluorobenzoic acid (3.2 g) is added thiony chloride (7 ml) and the mixture is refluxed for 1 hour. After concentrating, 2-methyl-3,4,6-trifluorobenzoyl chloride (3.3 g) is obtained.

Source