Réaction #1340985

ord-97861cdbba264fa08a02ab3beb1a0df5

Équation de réaction

Cc1ccc(S(=O)(=O)OCCC(C)(C)O)cc1
3-hydroxy-3-methylbutyl 4-methylbenzenesulfonate
Cc1cc(O)cc(C)c1Br
4-bromo-3,5-dimethylphenol
Cc1cc(OCCC(C)(C)O)cc(C)c1Br
compound
Rendement 0.1%
Cc1cc(OCCC(C)(C)O)cc(C)c1Br
4-(4-bromo-3,5-dimethylphenoxy)-2-methylbutan-2-ol
Rendement 0.1%

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

According to the method of (Example 36) <Step 1>, from 3-hydroxy-3-methylbutyl 4-methylbenzenesulfonate (5.1 g) and 4-bromo-3,5-dimethylphenol (3.6 g), the subject compound (5.2 mg) was obtained as a colorless oil.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US08455500B2uspto-grants-2013_06