Réaction #1256724

ord-8ab2b15329334edda2b86425c20bd320

Équation de réaction

CCCC1CCc2c(c(=O)oc3cc(OCC)ccc23)C1
3-ethoxy-8-propyl-7,8,9,10-tetrahydrobenzo[c]-chromen-6-one
CCCC1CCC2c3ccc(OCC)cc3OC(=O)C2C1
3-ethoxy-8-propyl-6a,7,8,9,10,10a-hexahydrobenzo[c]chromen-6-one

Solvants

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Traitement

  1. 1
    FiltrationThe solution is filtered
  2. 2
    Autreevaporated

Mode opératoire

8.60 g (30 mmol) of 3-ethoxy-8-propyl-7,8,9,10-tetrahydrobenzo[c]-chromen-6-one are dissolved in THF and hydrogenated to cessation on palladium/active carbon. The solution is filtered and evaporated, giving 3-ethoxy-8-propyl-6a,7,8,9,10,10a-hexahydrobenzo[c]chromen-6-one as colourless oil.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US07824745B2uspto-grants-2010_11