Réaction #1166493

Équation de réaction

4-nitrobenzylphosphonic acid

2-methyl-1,3-propanediol

→

5-methyl-2-(4-nitrobenzyl)-1,3,2-dioxaphosphorinane-2-oxide

Conditions de réaction

Mode opératoire

With 4-nitrobenzylphosphonic acid and 2-methyl-1,3-propanediol, the same procedure as in Reference Example 11 was followed, to yield 5-methyl-2-(4-nitrobenzyl)-1,3,2-dioxaphosphorinane-2-oxide, which was then recrystallized from ethanol-hexane to yield colorless prisms having a melting point of170° to 171° C.

Source