Réaction #1147965

Équation de réaction

2-(2-(2-methoxyethoxy)-ethoxy)-ethoxy-acetic acid

chloromethyl chlorosulfate

→

Chloromethyl 2-(2-(2-methoxyethoxy)-ethoxy)-ethoxy-acetate

Conditions de réaction

Traitement

1. 1
   workup.DISTILLATIONThe resulting oil was purified by distillation in vacuo, b.p.: 130-132° C. at 0.06 mbar

Mode opératoire

This compound was prepared from 2-(2-(2-methoxyethoxy)-ethoxy)-ethoxy-acetic acid and chloromethyl chlorosulfate as described in the general procedure given in Synthetic Communications 14, 857-864 (1984). The resulting oil was purified by distillation in vacuo, b.p.: 130-132° C. at 0.06 mbar.

Source