Réaction #11389

ord-ed84d5940c3742fc961e388b67925154

Équation de réaction

O=C(O)c1cn(-c2ccc(F)cc2F)c2cc(F)c(F)cc2c1=O
1-(2′,4′-difluorophenyl)-6,7-difluoro-1,4-dihydro-4-oxo-quinoline-3-carboxylic acid
CC1CNCC(C)C1
3,5-dimethylpiperidine
CC1CC(C)CN(c2cc3c(cc2F)c(=O)c(C(=O)O)cn3-c2ccc(F)cc2F)C1
titled product
Rendement 43.0%
CC1CC(C)CN(c2cc3c(cc2F)c(=O)c(C(=O)O)cn3-c2ccc(F)cc2F)C1
1-(2′,4′-Difluorophenyl)-6-fluoro-1,4-dihydro-7-(3′,5′-dimethylpiperidin-1-yl)-4-oxo-quinoline-3-carboxylic acid
Rendement 43.0%

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

The condensation of with 1-(2′,4′-difluorophenyl)-6,7-difluoro-1,4-dihydro-4-oxo-quinoline-3-carboxylic acid with 3,5-dimethylpiperidine in a similar manner as described in example 1 gave the titled product. Yield 43%, m.p 224–26° C., C23H21F3N2O3, m/z 431. (M+1)

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US07098219B2uspto-grants-2006_08